Simultaneous residue analysis of neonicotinoid insecticides in honey using LC-MS/MS

• 발행기관: 한국예방수의학회
• 저자명: Su Min Nam Jin Hyang Bae Do Hui Kim Hwan Goo Kang
• 간행물 정보: 『Journal of Preventive Veterinary Medicine』Vol.48, No.4, 262~269쪽, 전체 8쪽
• 주제분류: 의약학 > 기타의약학
• 파일형태: PDF
• 발행일자: 2024.12.31

국문 초록

In this study, an simultaneous LC-MS/MS multi-residue analytical method was developed and validated for the residues of six neonicotinoid insecticides (acetamiprid, clothianidin, dinotefuran, imidacloprid, thiacloprid, and thiamethoxam) in honey. Sample preparation included a combination of QuEChERS extraction kit and liquid-liquid extraction method to effectively extract pesticide components from the honey matrix and optimized analytical conditions to achieve high sensitivity and selectivity. The limits of detection (LOD) and the limits of quantitation (LOQ) were set in the range of 6-15 ng/mL and 19-44 ng/mL, respectively and the correlation coefficient (R²) was greater than 0.99, confirming good linearity. In addition, the intra-day recoveries for each pesticide were 75-104%, and the coefficient of variation (CV) was less than 20%, which met the guideline recommended by the Ministry of Food and Drug Safety. The LC-MS/MS method developed in this study is expected to be used as a multi-residue analysis method for 6 neonicotinoid pesticides in honey.

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키워드

Neonicotinoid insecticides Honey Analysis LC-MS/MS

참고문헌

• Sci Total Environ
• EFSA Journal
• Food Chem
• J Chromatogr B Analyt Technol Biomed Life Sci
• Environ Res
• Molecules
• LWT
• J Agric Food Chem
• Plos One