In-Situ Transmission Electron Microscopy Experiments

Renu Sharma 지음

Wiley-VCH 2023년 05월 09일 출간

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In-Situ Transmission Electron Microscopy Experiments Design and execute cutting-edge experiments with transmission electron microscopy using this essential guide In-situ microscopy is a recently-discovered and rapidly-developing approach to transmission electron microscopy (TEM) that allows for the study of atomic and/or molecular changes and processes while they are in progress. Experimental specimens are subjected to stimuli that replicate near real-world conditions and their effects are observed at a previously unprecedented scale. Though in-situ microscopy is becoming an increasingly important approach to TEM, there are no current texts combining an up-to-date overview of this cutting-edge set of techniques with the experience of in-situ TEM professionals. In-Situ Transmission Electron Microscopy Experiments meets this need with a work that synthesizes the collective experience of myriad collaborators. It constitutes a comprehensive guide for planning and performing in-situ TEM measurements, incorporating both fundamental principles and novel techniques. Its combination of technical detail and practical how-to advice makes it an indispensable introduction to this area of research. In-Situ Transmission Electron Microscopy Experiments readers will also find: Coverage of the entire experimental process, from method selection to experiment design to measurement and data analysis Detailed treatment of multimodal and correlative microscopy, data processing and machine learning, and more Discussion of future challenges and opportunities facing this field of research In-Situ Transmission Electron Microscopy Experiments is essential for graduate students, post-doctoral fellows, and early career researchers entering the field of in-situ TEM.

목차

Table of Contents CHAPTER 1 INTRODUCTION 1.1 Scope of the Book 1.2 Review of the Chapters CHAPTER 2 FUNDAMENTALS OF ELECTRON MICROSCOPY 2.1 Overview of Electron Optics 2.2 General functioning and applications of TEM/STEM CHAPTER 3 IMPACT AND LIMITATIONS OF IN-SITU TECHNIQUES 3.1 Potential Benefits of Performing an In situ TEM experiment 3.2 Potential Limitations and Cautions of Performing an In situ TEM experiment CHAPTER 4 GENERAL MICROSCOPE SELECTION AND STAGE DESIGN PHILOSOPHY 4.1 Microscope Selection 4.2 Stage Design Philosophy 4.3 Image Recording Techniques CHAPTER 5 IN SITU DEFORMATION 5.1 Qualitative Loading 5.2 Quantitative Loading CHAPTER 6 IN SITU HEATING 6.1 Classical Conductive Heating 6.2 MEMS Conductive Heating 6.3 Convective Heating 6.4 Radiative Heating CHAPTER 7 IN SITU COOLING 7.1 Peltier Cooling 7.2 Cryogenic Cooling CHAPTER 8 IN SITU CHARGED PARTICLE RADIATION 8.1 Electron Irradiation 8.2 Ion Irradiation CHAPTER 9 IN-SITU GAS-SOLID REACTIONS 9.1 Environmental Stages 9.2 Environmental Microscopes CHAPTER 10 IN SITU LIQUID-SOLID INTERACTIONS 10.1 Ionic Liquids and Closed Liquid Cell 10.2 Microfluidic Design Chapter 11 IN SITU EM FIELD EFFECTS 11.1 Electrical Biasing 11.2 Dynamic Lorentz Imaging Chapter 12 DYNAMIC AND ULTRA-FAST TEM 12.1 Dynamic TEM 12.2 Ultra-fast TEM CHAPTER 13 COUPLING OF IN SITU TEM TECHNIQUES 13.1 Coupling within the listed approaches 13.2 Coupling to other Structure and Property CHAPTER 14 DATA HANDLING AND PROCESSING 14.1 Data Collection 14.2 Data Processing 14.3 Data Storage CHAPTER 15 FUTURE DIRECTION OF IN SITU TEM TECHNIQUES

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저자(글) Renu Sharma