Environmental Trace Analysis

John R. Dean 지음

Wiley 2013년 10월 10일 출간

작품소개

책소개

Thisbook covers all aspects of environmental trace analysis from sampling through to preparation of the sample to the analytical techniques used to quantify the level of trace metals or organic compounds. The book is divided into two areas: sample preparation for inorganic analysis and sample preparation for organic analysis. This allows the reader to focus on key aspects related to the preparation of samples for their subsequent analysis. Selected case studies provide the reader with the opportunity to consider how the sample preparation approach can be optimized for their own area of expertise.

목차

About the Author xvPreface xviiAcknowledgements xixAcronyms and Abbreviations xxi1 Basic Laboratory Procedures 11.1 Introduction 11.2 Health and Safety Issues 21.3 Sample Handling: Solid Samples 41.4 Sample Handling: Liquid Samples 41.5 Sample Handling: Gases/Vapour Samples 51.6 Summary 52 Investigative Approach for Environmental Analysis 72.1 Introduction 72.2 Recording of Practical Results 72.3 Significant Figures 92.4 Units 122.5 Summary 133 Principles of Quantitative Environmental Analysis 213.1 Introduction 213.2 Preparing Solutions for Quantitative Work 233.3 Calibration Graphs 243.4 Limits of Detection/Quantitation 273.5 Calculations: Dilution or Concentration Factors 273.6 Quality Assurance 293.7 Summary 364 Environmental Sampling 374.1 Introduction 374.2 Sampling Soil (and Sediments) 394.3 Sampling Water 404.4 Sampling Air 424.5 Summary 445 Storage of Samples for Analysis 455.1 Introduction 455.2 Choice of Storage Container for Liquid Samples 455.3 Preservation Techniques for Liquid Samples 475.4 Storage and Preservation of Solid Samples 485.5 Storage and Preservation of Gaseous Samples 485.6 Summary 506 Preparation of Environmental Solid Samples for Inorganic Analysis 516.1 Introduction 516.2 Decomposition Techniques 536.3 Selective Extraction Methods 646.4 Physiologically-Based Extraction Test or In Vitro Gastrointestinal Extraction 706.5 Earthworms 726.6 Summary 757 Preparation of Environmental Liquid Samples for Inorganic Analysis 817.1 Introduction 817.2 Liquid-Liquid Extraction of Metals 827.3 Ion Exchange 837.4 Co-precipitation 847.5 Summary 848

작가정보

저자(글) John R. Dean

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Professor John Dean, Professor of Analytical and Environmental Science, Northumbria University, UKFellow of the Royal Society of Chemistry (FRSC); Chartered Chemist (C.Chem.); Chartered Scientist (C.Sci.); Registered Analytical ChemistJohn Dean's recent research work has focused on (a) the application of the physiologically-based extraction test to assess environmental health risk from metals and polycyclic aromatic hydrocarbons in contaminated land studies, (b) development of new high performance liquid chromatographic approaches for environmental and pharmaceutical compounds, and, (c) development of novel gas chromatographic approaches as a diagnostic tool for bacterial detection/identification.